Microscopy lab laboratories with MicroVision Laboratories 2021? Approach: MicroVision Labs’ staff consulted with the client, and determined that, unfortunately, there could be a number of potential sources of a white material. Even before the bottle with the suspended material arrived, it was determined that there was less than 50 mL of water remaining, and likely less than a gram of material suspended in the water. The client was aware that this material could represent precipitated minerals from the source water, a polymer residue from the bottles, some form of biological tissue that might have formed despite sterilization procedures, or could very well represent some completely unforeseen foreign material. The issue facing the client is how to have the material tested, as most tests that they might request for one or the other of these known potential sources would destroy or alter the sample. Choosing a test was therefore something of a gamble, because if they tested for calcium (mineral precipitate) and it came up negative – that didn’t actually tell them what the powder was, just that it didn’t have any calcium. Based on this conversation, the non-destructive, specialized testing at MicroVision Laboratories was chosen as the best choice.
Energy Dispersive Spectroscopy (EDS) identifies the elements present in a sample by analyzing the X-rays generated by the electron beam of the Scanning Electron Microscope (SEM), making it an indispensable tool. Since X-rays are only generated from the area of the surface excited by the small electron beam, spectra of individual areas or particles can be obtained. Spectral information can therefore be generated for an entire field of view by scanning the beam, providing an elemental map. With the high count rate and excellent signal to noise ratio of our advanced QDD EDS detectors, high resolution data sets are collected and analyzed in minutes, rather than days. This elemental mapping technique allows our clients to immediately visualize the chemical landscape in their samples. Additionally, since the entire spectra is stored for each pixel, areas of interest that are identified later can be examined in detail, without ever having to re-image the sample. Other labs can’t touch the quality and visual impact of the elemental maps we produce here at MicroVision Labs.
How do I submit a sample or a set of samples? To submit a sample or set of samples, please see the page How to Submit Samples. What if I believe my samples are hazardous? We are not equipped to handle or dispose of every kind of hazardous material. Please call us before sending in any potentially hazardous samples. In cases where we are able to analyze your harzardous samples we may not be able to dispose of them and therefore we will return them to you. Read a few more info on click here for more info. We are proud to announce that MicroVision Labs is now accredited to the ISO/IEC 17025:2017 standard. This represents over a year of diligent effort from all of our staff to verify and validate our in house SOP’s and transform our quality management system to one that is compliant to this international standard. This certification requires that accredited labs demonstrate that they are competent and can produce technically valid data and results unlike other certifications such as ISO 9001:2015. This represents an obvious value to our clients.
Close examination of any possible defects or voids was undertaken at higher magnification. The voids did not appear to create any structural or conductivity issues. Additionally, the formation and contiguity of intermetallic bonds between the contacts and solder were shown using a combination of EDS line scan elemental spectroscopy and elemental mapping. The SEM image and the EDS map to the left show the intermetallic layer between the copper wire and the tin/lead solder via the mixture of the red copper and the blue tin.
The client was able to determine the source of the black dust was due to the mechanical breakdown of the foam cushions in the impacted room, and not from mold or mildew growth. The experienced analysts at MicroVision Labs were able to differentiate the foam materials from either blown cellulose or urethane foam insulation or air filters, allowing for the client to easily remove the problem cushions. See even more info on this website.